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Préparation d’échantillons (SPE)

preparation echantillons SPELa gamme de produits d’extraction Cleanert a été conçue pour simplifier et améliorer vos préparations d’échantillons en combinant supports, formats et méthodologies appropriées. Ces produits utilisent différents types de supports (Silices nues ou greffées, Polymères,Fluorisil, Carbone…) pour préparer tous types d’échantillons. Les cartouches Cleanert présentent une grande pureté, stabilité ainsi qu’une excellente reproductibilité.

Avec les produits Cleanert vous bénéficirez de méthodes SPE robustes sans devoir craindre l’obtention de résultats non reproductibles ni de faibles rendements.

Silice greffée

Cleanert ODS C18

ODS C18 cartridges and plates are packed with reversed phase, octadecylsilane
bonded silica sorbents. The sorbent is double endcapped and has a high bonding
density (%C>17). These cartridges can be used as a replacement for BondElute C18
and Super clean ENVI C18. These products can be used for desalting biomolecules,
such as proteins and DNAs.

  • Based on silica; C%: 18-19%
  • Average particle diameter: 50µm
  • Average pore size: 60Å
  • Volume of pore: 0.8cm²/g
  • Specific surface area: 480²/g.

Cleanert ODS C18-N

ODS C18-N products have silica based reverse phase sorbents bonded with
octadecylsilane without endcapping. The extra silanol residue of the sorbent
provides additional polar interactions associated with surface silanol
groups which enhance the retention of basic compounds. These columns are
similar to Agilent AccuBond C18 and BondElute C18 OH.

  • Based on silica; C%: 17-18%
  • Average particle diameter: 50µm
  • Average pore size: 60Å
  • Volume of pore: 0.8cm²/g
  • Specific surface area: 480²/g

Cleanert C8

The property of C8 products is similar to ODS C18 products. However,
this sorbent is slightly less retentive than C18, which facilitates the elution
of more hydrophobic substance. C8 is successfully used for the extraction of both
water-soluble and fat-soluble vitamins from serum, as well as the desalting of biological
macromolecules.

  • Based on silica; C%: 9-10%
  • Average particle diameter: 50µm
  • Average pore size: 60Å
  • Volume of pore: 0.8cm²/g
  • Specific surface area: 480²/g

Cleanert CN

Cleanert CN(cyano-)SPE cartridge is cyanopropyl-boned-silica based extraction cartridge.
This cartridge is with medium polarity, and can be used for reversed phase or normal phase
extraction.

Cleanert NH2

NH2 SPE products have silica based sorbents bonded with aminopropyl funtional group.
This sorbent can be used in either normal phase or reverse phase mode. It retains the
analytes either by a polar adsorption (from non-polar solution) or by weak anion exchange
(from aqueous solution). pKa=9.8 .

  • Based on silica
  • Average particle diameter: 50µm
  • Average pore size: 60Å
  • Volume of pore: 0.8cm²/g
  • Specific surface area: 480m²/g

Cleanert COOH

COOH SPE products consist of a propane carboxylic acid on the inner silica surface.
The pKa of the carboxylic acid group is approximately 3.8. It is a useful sorbent for
quaternary ammonium salt and other strong cations.

  • Based on silica; C%: 5-6%
  • Average particle diameter: 50µm
  • Average pore size: 60Å
  • Volume of pore: 0.8cm²/g
  • Specific surface area: 4802/g

Cleanert Silica

Silica SPE product has unbonded, activated irregular silica as the sorbent.
This sorbent exhibits high polar interaction and is used for the extraction of
weak-polar or non-polar compound, such as oil. In addition, the silanol groups
are ionzable at intermediate pH, so it can be used as a weak cation exchanger.

  • Based on silica;
  • Average particle diameter: 50µm;
  • Average pore size: 60Å;
  • Volume of pore: 0.8cm2/g;
  • Specific surface area: 4802/g

Cleanert PSA

PSA SPE is similar to Cleanert-NH2. PSA has two amino groups with pKa=10.1
and 10.9 respectively. This sorbent is an anion exchanger slightly stronger
than NH2. It can be used for the extraction of metal ions by chelating interactions.
It is also commonly used to remove organic acids, pigments and metal ions from organic
samples such as vegetables and fruits.

  • Based on silica
  • Average particle diameter: 50µm
  • Average pore size: 60Å
  • Volume of pore: 0.8cm²/g
  • Specific surface area: 480²/g

Cleanert PRS

PRS SPE sorbent is a silica gel based strong cation exchanger. This sorbent,
consisting of a propane sulfonic acid, has slightly less exchange capability than SCX.
It can be applied to the extraction of weak cations, such as pyridine, with high recovery.

  • Based on silica;
  • Average particle diameter: 50µm;
  • Average pore size: 60Å;
  • Volume of pore: 0.8cm2/g;
  • Specific surface area: 480m2/g
  • The ion exchange degree: 0.3meq/g.

Cleanert SCX

SCX products are strong cation exchangers based on silica gel, with benzene
sulfonic acid. The sorbent is used to extract positively charged basic compounds
or remove the salt from biological samples. It can also be mixed with C18 sorbent
to extract the organic bases.

  • Based on silica;
  • Average particle diameter: 50µm;
  • Average pore size: 60Å;
  • Volume of pore: 0.8cm2/g; Specific surface area: 480m2/g
  • The ion exchange degree: 0.5meq/g.

Cleanert SAX

SAX SPE products have silica based sorbents bonded with a quaternary amine. This strong
anion exchanger is used to extract compounds capable of carrying a negative charge from both
aqueous and non-aqueous solutions. They are ideally suit to extraction of weak acids and desalting
of biological macromolecules, like BondElute-SAX.

  • Based on silica; C%: 9-10%;
  • Average particle diameter: 50µm;
  • Average pore size: 60Å;
  • Volume of pore: 0.8cm2/g;
  • Specific surface area: 480m2/g
  • The ion exchange degree: 0.5meq/g.

Cleanert Diol

Silica based dihydroxy SPE. It is used to extract polar analytes from non-polar solutions.
It is a neutral sorbent and extracts compounds by forming hydrogen bonding or polar-polar
interaction. As an example, it can be used to extract THC.

  • Based on silica; C%: 5-6%;
  • Average particle diameter: 50µm;
  • Average pore size: 60Å;
  • Volume of pore: 0.8cm2/g;
  • Specific surface area: 4802/g
Sorbent Vol. Tubes/box ODS C18 (end capping) ODS C18 (without end capping) C8 CN NH2 PSA
100mg 1ml 100 181001 181001-N 081001 CN1001 NH1001 PA1001
200mg 3ml 50 182003 182003-N 082003 CN2003 NH2003 PA2003
500mg 3ml 50 185006 185006-N 085006 CN5006 NH5006 PA5006
500mg 6ml 30 180006 180006-N 080006 CNOO06 NHOO06 PAOO06
1g 6ml 30 180100 180100-N 080100 CN0100 NH0100 PAO 1 00
50mg/well 2ml 30 180502-W 180502-N-W 080502-W CN0502-W NH0502-W PA0502-W
100mg/well 2ml 30 181002-W 181002-N-W 081002-W CN1002-W NH1002-W PA1002-W
10g 180010 180010-N 80010 CN0010 NH0010 PA0010
100g 180100 1810100-N 80100 CN0100 NH0100 PA0100
Sorbent Vol. Tubes/box SAX COOH PRS SCX Silica Diol
100mg 1ml 100 SA1001 CH1001 PR1001 8C1001 811001 010501
200mg 3ml 50 SA2003 CH2003 PR2003 8C2003 812003 011001
500mg 3ml 50 SAS006 CH5006 PR5006 8C5006 815006 015006
500mg 6ml 30 SAOO06 CHOO06 PROO06 8COO06 810006 010006
1g 6ml 30 SA0100 CH0100 PR0100 8C0100 810100 010100
50mg/well 2ml 30 SA0502-W CH0502-W PR0502-W 8C0502-W 810502-W 010502-W
100mg/well 2ml 30 SA1002-W CH1002-W PR1002-W 8C1002-W 811002-W 011002-W
10g SA0010 CH0010 PR0010 SC0010 SI0010 DI0010
100g SA0100 CH0100 PR0100 SC0100 SI0100 DI0100

Support d'absorption sans silice

Cleanert Alumina A

Cleanert Alumina A is acidic alumina SPE cartridge, the pH of which is 4.5.
It can be used as strong polar adsorbent and medium cation exchanger. The special
deactivation of this cartridge makes sure the reproducibility of samples.

Cleanert Alumina B

Alumina B products(pH=10) can be used to remove organic acids and phenols in the
sample matrix. They have been pre-treated by special deactivation to ensure high
analytes recovery.

  • Adsorption sorbents
  • Average particle size: 150 mesh
  • Average pore size: 58Å

Cleanert Alumina N

Alumina N sorbents(pH=7.5) can adsorb molecules by interaction with the aluminum
metal center. The neutralized surface allows interaction with compounds whose heteroatoms
are electronegative(e.g.N,S,P) or with an electron-rich ,highly aromatic structure.

  • Adsorption sorbents
  • Average particle size: 150 mesh
  • Average pore size: 58Å

Cleanert Pesticarb

PestiCarb is made of graphitized carbon by a distinct surface modifcation process, and has been
used for sample cleanup in pesticide residues in plants or animal tissues. This sorbent can effectively
reduce the background noise and increase the sensitivity, the functions of which are similar to Supelco
Envicarb.

  • Adsorption sorbents
  • Average particle size: 120-400 mesh.
Sorbent Vol. Tubes/box Florisil PestiCarb Alumina N Alumina A Alumina B
100mg 1ml 100 FS1001 PC1001 AL1001-N AL1001-A AL1001-B
200mg 3ml 50 FS2003 PC2506 AL2003-N AL2003-A AL2003-B
500mg 3ml 50 FS5006 PC5006 AL5006-N AL5006-A AL5006-B
500mg 6ml 30 FS0006 PCOO010 AL0006-N ALOO06-A AL0006-B
1g 6ml 30 FS0100 PC200010 ALOIOO-N AL0100-A AL0100-B
50mg/well 2ml 30 FS0502-W PC0502-W AL0502-N-W AL0502-A-W AL0502-B-W
100mg/well 2ml 30 FS1002-W PC1002-W AL1002-N-W AL1002-A-W AL1002-B-W
10g FS0010 PC0010 AL0010-N AL0010-A AL0010-B
100g FS0100 PC0100 AL0100-N AL0100-A AL0100-B

Polymères

Cleanert PEP

PEP is made of polydivinylbenzene on which the surface is functionalized with vinyl prolidone.
The material has a balanced hydrophilic and hydrophobic property and can be used in the entire
pH range of 1-14.

  • Functionalized polymer sorbents
  • Average particle size: 35µm or 70µm.
  • Average pore size: 80Å
  • Surface area: 600m2/g.

Cleanert PEP-2

Cleanert PEP-2(Polar Enhanced Polymer)is functional polystyrene/divinylbenzene SPE cartridge. The surface
is bonded with hydrophilic and hydrophobic functional groups simultaneously. So this cartridge has equivalent
adsorption interaction with polar or non-polar compounds. The applicable pH range is 1.0-14.0. It is equivalent
to Waters Oasis HLB.

Cleanert PEP-H

PEP-H is one of the series of PEP.

It is base on the polydivinylbenzene and derived from PEP by increase the surface polarity
to improve the adsorption for polar analytes

The material can be used in the entire pH range of 1-14, also can be used to extract a variety
of polar and non-polar compounds. Some highly hydrophilic compounds
which have little retention on C18 columns

  • Functionalized polymer sorbents
  • Average particle size: 70µm.
  • Average pore size: 80Å
  • Surface area: 600m2/g

Cleanert PCX

Cleanert PCX is water-wettable polymer based SPE cartridge, which
depends on cation exchange mixed mechanism. It is stable in the pH range
of 0-14.0. In addition, this cartridge has high binding capacity. It is widely
used for extraction and purification of basic compounds from biological matrices,
which need high adsorption capacity, such as plasma, urine, bile, tissue homogenate.

It is equivalent to Waters Oasis MCX.

Cleanert PAX

It is designed to overcome the limitations of traditional silica based mixed-mode SPE sorbents such
as C18/SAX. It is a RP/strong anionexchange mixed mode polystyrene/divinylbenzene sorbent, stable
from pH 0-14.0 .

  • Based on functioalized polystyrene/divinylbenzene
  • Average particle diameter: 40µm
  • Average pore size: 70Å
  • Volume of pore: 1.2cm2/g
  • Specific surface area: 6002/g

Cleanert PWCX

Cleanert PWCX provides the dual modes of retention, weak cation exchange and reverse
phase on a stable polymer sorbent, which improves the retention for basic analytes.

  • Based on partially functionalized polystyrene/divinylbenzene;
  • Average particle diameter: 40µm
  • Average pore size: 70Å
  • Volume of pore: 1.2cm2/g
  • Specific surface area: 6002/g.

Cleanert PWAX

Cleanert PWAX provides the dual modes of retention, weak anion exchange and
reverse phase on a stable polymer sorbent, which improves the retention for
acidic analytes.

  • Based on partially functionalized aminopolystyrene/divinylbenzene
  • Average particle diameter: 40µm
  • Average pore size: 70Å
  • Volume of pore: 1.2cm2/g
  • Specific surface area: 6002/g.

Cleanert PS

PS is made of non-substituted polydivinylbenzene. It has larger surface areas (>600m2/g.) and thus greater capacity
than reverse phase bonded silica.PS can be used for the extraction of non-polar and polar compounds.

  • Based on polystyrene/divinylbenzene
  • Average particle diameter: 40µm
  • Average pore size: 70Å
  • Volume of pore: 1.2cm2/g
  • Specific surface area: 6002/g.
Sorbent Vol. Particle Size Tubes/box PEP PEP-2 PEP-H PAX PCX PWAX PWCX PS
30mg 1ml 35µm 100 PE0301-S
60mg 3ml 35µm 50 PE0603-S
30mg 1ml 70µm 100 PE0301 PE0301-2 PE0301-H AX0301 CX0301 WA0301 WC0301 PS0301
60mg 3ml 70µm 50 PE0603 PE0603-2 PE0603-H AX0601 CX0601 WA0603 WC0603 PS0601
100mg 3ml 70µm 50 PE1003 PE1003-2 PE1003-H AX0603 CX0603 WA1003 WC1003 PS0603
200mg 6ml 70µm 30 PE2006 PE2006-2 PE2006-H AX1506 CX1506 WA2006 WC2006 PSI508
500mg 6ml 70µm 30 PE5006 PE5006-2 PE5006-H AX5006 CX5006 WA5006 WC5006 PS5008
30mg/well 2ml 70µm 96-wellplate PE0302-W PE0302-2W PE0302-HW AX0302-W CX0302-W WA0302-W WC0302-W PSQ302-W
50mg/well 2ml 70µm 96-wellplate PE0502-W PE0502-2W PE0502-HW AX0502-W CX0502-W WA0502-W WCOOO2-W PSQ502-W
10g 70µm PE0010 PE0010-2 PE0010-H AX0010 CX0010 WAOOIO WCOOI0 PSOO10
100g 70µm PE0100 PE0100-2 PE0100-H AX0100 CX0100 WA0100 WC0100 PS0100
30mg/well 2ml 35µm 96-wellplate PE0302-SW
50mg/well 2ml 35µm 96-wellplate PE0502-SW
10g 35µm PE0010-S
100g 35µm PE0100-S

Phases spéciales

Cleanert HXH

HXN is also made of polydivinylbenzene having surface modified with vinylpyrrolidone.
This sorbent is specially designed to extract sulfonyl ureas from water and soil at ppb level.
It is less polar than PEP and can also be used to extract, enrich and clean up samples from
mid polar to high polar compounds.

  • Based on polystyrene/divinylbenzene;
  • Average particle diameter: 40µm;
  • Average pore size: 70Å;
  • Volume of pore: 1.2cm2/g;
  • Specific surface area: 6002/g
Sorbent Vol. Tubes/box HXN
30mg 1mL 100 HX0301
60mg 3mL 50 HX0603
100mg 3mL 50 HX1003
200mg 6mL 30 HX2006
500mg 6mL 30 HX5006
30mg/well 2mL 96w HX0302-W
50mg/well 2mL 96w HX0502-W
10g HX0010
100g HX0100

Cleanert SUL-5

Specific SPE column for Sulfonamides

SUL-5(Specific SPE column for Sulfonamides) is specially designed
for the extraction of five sulfonamides (SM2, SMM,SMZ, SDM, SQ) in p

Sorbent Vol. Tubes/box HXN
2g 12ml 100 SUL-5

Cleanert DNPH-Silica

Specialized for Pretreatment of Aldehydes and Ketones in Air

At least 14 species of aldehydes and ketones compounds can be detected,
including formaldehyde, acetaldehyde, propionaldehyde, acrolein, butyraldehyde,
E aldehyde, isoamyl aldehyde, hexanal, benzaldehyde, o,m,p-methyl Benzaldehyde,
2,5-dimethyl benzaldehyde, acetone, butanone, pentanone, cyclohexanone, acetophenone.

(1) the average background value of technical indicators: = 0.2µg. (As formaldehyde)
Maximum sample volume :> 75µg. (As formaldehyde)
Maximum sample pressure: 0.15MPa.
The recovery:>90%.

(2) Storage conditions: low temperature (4 ?) and from light
Shelf Life: 90 days.

Notice:Use as soon as possible after unpacking.

Sorbent Vol. Tubes/box DNPH
200mg 3ml 1 DN2003
200mg 1ml 1 ICDN2001

Cleanert TPH

TPH means triple phase SPE for Herb, and it was constituted by three kinds of materials.
These three kinds of materials using different mechanism of action, focus on the colorants,
organic acid and organic substance, also cosidering different polarity of the interferent,
such as nonpolarity substance, substance with hydroxyl and carboxyl group, also the basic group.
By mixing different materials together, we achieve a better result of clean up, expecially complicated matrix.

TPH is majorly used for extraction and detection of pesticides from ChineseHerb such as Ramulus Mori,
Honeysuckle and the Fruit of Chinese Wolfberry, It can absorb reduce up to 80% interferent and without adsorb
any pesticide residues.

Cleanert TPH has been used in China national standard methods, Determination of 488 Pesticide Residues
and Related Chemicals Residues and 413 Pesticide Residues and Related Chemicals Residues in the Ramulus Mori,
Honeysuckle and the Fruit of Chinese Wolfberry with GS-MS and LC-MS/MS Respectively, Determination of 448 pesticides
and related chemicals residues in tea—LC-MS-MS method. The process mainly containing ACN extraction, Load the
sample on the pre-actived column, and then eluted by ACN- toluene (3+1).

Sorbent Vol. Tubes/box TPH
1g 6ml 30 TPH0006
2g 12ml 20 TPH200010

Cleanert TPT

TPT was constituted by three kinds of materials. These three kinds of materials using different
mechanism of action, focus on the colorants, organic acid and tea polyphenols, also cosidering different
polarity of the interferent, such as nonpolarity substance, substance with hydroxyl and carboxyl group,
also the basic group. By mixing different materials together, we achieve a better result of clean up,
expecially complicated matrix. TPT is majorly used for extraction and detection of pesticides from tea
leaf, It can adsorb reduce up to 80% interferent and without adsorbing any pesticide residues.

Sorbent Vol. Tubes/box TPT
1g 6ml 30 TPT0006
2g 12ml 20 TPT200010

Cleanert EPH

Cleanert EPH use specially silica as material to separate aliphatic fraction to atomatic fraction
in soil. The column was used in New Jersey Department of Environmental Protection Site Remediation Program,
extractable petroleum hydrocarbons methodology (Version 1.1). The method also can be move onto the SPE working
station of full-automatic (SPE-10 P/N: SPE-10).

Sorbent Vol. Tubes/box EPH
5g 25ml 15 SI500025-30

Cleanert PPP

Protein Precipitation Plate

Cleanert Protein Precipitation Plate product for DMPK research is manufactured
with the reagents of the highest purity. Every lot is subjected to a wide range of
rigorous quality control tests and must confrm to our strict specifcation.The graded
frit design is optimized to efficiently remove most of the interference of plasma
samples without plugging or breakthrough.The 96-well plate design can be accomplished
with most of auto-station, also minimizing sample handling. The plates are compatible
with Agela 96 well vacuum manifold, also can be used in centrifugal machine.

Loading about 50µl plasma sample

  • Add 3 times solvents(ACN:Methanol =3:1)as elute solution and shake the plate to help precipitation
  • Apply vacuum or centrifuge to get the solution through the plate
Sorbent Vol. Tubes/box Vaccum Centrifuge
2ml 96wellplate 2 96CD2025 96CD2025-F

Cleanert LRC

Large Receiver Column

Cleanert LRC was design to load more solvents when SPE process,
specially can by used in little sorbent bed but Large elute solvents.

Sorbents Vol Tubes/Box Cleanert LRC C18 Cleanert LRC PEP
200mL 10mL 20 L1820010
260 mL 10mL 20 LPE0610

Cleanert LDC

Large Disk for water analysis Cartridge

Cleanert LDC use SPE sorbent to concentrated trace chemical substances in environmental samples.
The special cartridge design was suitable for water concentration, and it can replace SPE disk
in most of the analysis.

Meterial Vol Tubes/Box Cat.No
Cleanert LDC C18 100 4 L181500100
Cleanert LDC C18 100 4 L181500100-N
Cleanert LDC PEP 100 4 LPE000100
Cleanert LDC PS 100 4 LPS000100
Cleanert LDC SCX 100 4 LSC1500100

Cleanert Glass column

Cleanert Glass column series can reduce the dissolution of the tube material, and so can
be used in environmental analysis, especially the plasticizer and environmental interferent.

Meterial Vol Tubes/Box Cat.No
C18 glass 200 mL 3 mL 50 182003-G
Cleanert PEP glass 60mL 3 mL 50 PE0603-G

Rapid Test Strip

Rapid test strips for the detection of Aflatoxin,Voitoxin,Melamine,Clenbuterol,Ractopamine
in samples,such as milk,milk powder,feed,cheese,biscuit,urine,corn,rice,bean,peanut,wheat,peanut
butter

P/N Type Spec.  Sensitivity Application
BAQ09011 Melamine 50 /package 50ppb/100ppb milk,milk powder,feed,cheese,biscuit,urine
BAQ09005 Aflatoxin B1 50 /package 10ppb corn,rice,bean,peanut,wheat, feed
BAQ10001 Voitoxin 50 /package 100ppb corn,rice,bean,peanut,wheat,feed
BAQ09001 Clenbuterol(urine) 50 /package 3ppb swine urine
BAQ09001-1 Clenbuterol(tissue) 50 /package 1ppb swine urine,swine liver etc.
BAQ09002 Ractopamine(urine) 50 /package 3ppb swine urine
BAQ09002-1 Ractopamine(tissue) 50 /package 1ppb swine urine,swine liver etc.
BAQ09007 malachite green(water) 50 /package 2ppb water
BAQ09007-1 malachite green(tissue) 50 /package 2ppb tissue
BAQ09003 chlormycetin 50 /package 0.1ppb honey,milk,seafood,chicken

Phases mixtes

Cleanert C8/SCX

It is silica based, with mixed C8 and strong cation exchange chemical group. It is widely
used for extraction of basic drugs from urine and blood.

Sorbent Vol. Tubes/box C8/SCX
50mg 3ml 50 CS0503
130mg 3ml 50 CS1303
300mg 3ml 50 CS3003
500mg 6ml 30 CS5006
1g 6ml 30 CS0006
50mg/weel 6ml 96-wellplate CS0502-W
100mg/well 2ml 96-wellplate CS1002-W
10g CS0100
100g CS0101

PestiCarb/NH2

PestiCarb/NH2 SPE column is packed of 500mg PestiCarb and 500mg NH2.It has been used wildly
in analysis of pesticides residue, esp. for the Japanese Positive List System. It can be used
in pesticide residue analysis, coloring matter, fatty acid and hydroxybenzene.

Sorbent Vol. Tubes/box PestiCarb/NH2
500mg/500mg 6ml 30 PN0006

Phases MAS

MAS-C

Cleanert MAS is a simple sample treatment for bioanalysis which applies multi-function
impurity adsorption to remove as many as interferences. It combines protein precipitation
with SPE method, and achieve a faster and easier approach.

In LC/MS–(MS) bio-analysis, there are many interferences which will cause unsatisfied result,
such as protein, phospholipid, fat and some surfactant. Phospholipid is a main interference cannot
be eliminated enough by PPT, which can cause ion suppression and variation of peak shape and retation time.
Cleanert MAS follows the similar simple procedures of protein precipitation, but has a better efficency
of phospholipid removal.

Compared to traditional methods including liquid-liquid extraction (LLE), solid-phase extraction
(SPE) and protein precipitation (PPT), Cleanert MAS has a better performance on interference removal
and more convenient operation. It’s a better replacement of protein precipitation, also an evolution
of SPE.

MAS SPE cartridge
Spec. Application Package Part No.
1mL SPE cartridges, used for basic and neutral substances extraction in Plasma and biological samples 100 MSC-B-0301
1mL 100 MSC-B-0601
1mL SPE cartridges, used for acid substances extraction in Plasma and biological samples 100 MSC-A-0301
1mL 100 MSC-A-0601
MAS 96 well plate
Spec. Application Package Part No.
30mg/2ml/well 96 well plate, used for basic and neutral substances extraction in plasma and biological samples. 2 MS-B-0302W
30mg/2ml/well 96 well plate, used for basic and neutral substances extraction in plasma and biological samples, design with a filter membrane (can be used in centrifugation) 2 MS-B-0302W
30mg/2ml/well 96 well plate, used for acid substances extraction in plasma and biological samples. 2 MS-A-0302W
30mg/2ml/well 96 well plate, used for acid substances extraction in plasma and biological samples, design with a filter membrane (can be used in centrifugation). 2 MS-A-0302FW
30mg/2ml/well 96 well plate, used for weak acid substances extraction in plasma and biological samples. 2 MS-WA-0302-W
30mg/2ml/well 96 well plate, used for weak acid substances extraction in plasma and biological samples, design with a filter membrane (can be used in centrifugation) 2 MS-WA-0302-FW

MAS-Q

Adsorption of multiple mechanisms for impurity extraction purification method

Through multi-functionalized compound Absorption materials, biological samples will be
absorbed as the main interfere matrix, and strong water-soluble material be remained in the
tested samples solution. so as to achieve the purification and enrichment purposes

The General Method Includes

  • Put the samples and reagent in the centrifugal tube at the same
    time, vibration extraction and ultrasonic extraction.
  • Put SPE material in the centrifugal tube to purify the sample
    matrix and after centrifuging the analytes was remained in the solution.
  • Take supernatant for other treatment or direct detection
Sorbent Vol Tubes Description Cat.No
PAX 500mg, C18 500mg 50mL 50 MS-SPC5001
PAX 200mg , C18 200mg 50mL 50 MS-SPM5001
6g MgSO4(anhydrous), 1.5g NaAc.3H2O 50mL 50 Extraction tube, used in method(NYT-1380-2007), Apply to pesticide detection in the vegetables and fruit matrix MS-MG5050
100mg PSA,100mg C18, 0.3 g MgSO4(anhydrous) 15mL 50 Clean-up tube, used in method(NYT-1380-2007), Apply to pesticide detection in the vegetables and fruit matrix MS-PA1010
6g MgSO4(anhydrous),250mg PestiCarb,500mg NH2 50mL 50 Apply to pesticide detection in the vegetables and fruit matrix with lots of colorants MS-PN5050
magnesium sulfate 4 g; sodium chloride 1 g; sodium citrate dibasic sesquihydrate 0.5 g,sodium citrate tribasic dihydrate; 50 citrate extraction tube,use to extract the pesticides which are not stable in acid or basic solution MS-NMS5050
MgSO4, 750 mg 50 mL 50 PSA clean-up tube, used in purification of vegetable and fruit matrix MS-PAMG1550
PSA 125 mg
500mg C18 1.5mL 50 Get rid of fatty MS-185050
50mg C18, 150mg MgSO4 (anhydrous) 1.5mL 100 Get rid of fatty MS-180205
200mg PAX 10mL 100 Reduce protein and phospholipid(Basic substance) MS-AX1030
50mg PAX 1.5mL 100 MS-AX0230
200mg PCX 10mL 100 Reduce protein and phospholipid(Acid substance) MS-CX1030
50mg PCX 1.5 mL 100 MS-CX0230
200mg PEP 10mL 100 Reduce protein and phospholipid(Natural substance) MS-PE1020
50mg PEP 2mL 100 MS-PE0205

Phases IC

The sample preparation is necessary not only for HPLC but also for IC.

The demands for sample preparation of IC led to a development of a new SPE product family,
which we named « Cleanert Pre-IC”, and they can perform excellently for sample preparation of IC thanks to their sorbent of high capacity and a good flow property.

Cat.No The type of resin Average particle size Capacity Application Sepcification
IC-RP10 divinylbenzeneresin 40µm 300mg/1cccartridge To remove substances such as aromatic dyes, somearomatic carboxylic acids, hydrocarbons, andsurfactants from sample matrices. 50 pk
C-P10 polyvinylpyrrolidone(PVP) polymer resin 40µm 350mg/1cccartridge To remove the phenolic fraction of humic acids,tannic acids, lignins, anthocyanins, and azodyesfrom samples. 50 pk
IC-A10 16% cross-linked,styrene-based,anion-exchangeresin in thebicarbonate form. 40µm 0.7meq/1cccartridge To remove anion contaminant and neutralize thestrongly acidic sample solution.To remove high levels of alkaline ear 50 pk
IC-H10 16% cross-linked, styrene-based, sulfonic acid , cation-exchange resin in the hydrogen form 40µm 2.0-2.2meq/1cc cartridge To remove high levels of alkaline earths and transitionmetals from sample matrices and in the neutralizationof highly alkaline samples such as sodium hydroxideor sodium carbonate. 50 pk
IC-Ag10 16% cross-linked, styrene-based, sulfonic acid, cation-exchange resin in the silver form. 40µm 2.0-2.2meq/1cc cartridge To remove high levels of alkaline earths and transitionmetals from sample matrices without acidifying thesample. This ensures good recovery of acid labileanalytes such as nitrite. 50 pk
IC-Ba10 styrene-based, sulfonic acid , cation-exchange resin in the barium form. 40µm 2.0-2.2meq/1cc cartridge To remove SO42-.For reproducible, quantitativedeterminations in low-ionic-strength samples, thesecartridges should be activated with a chloride-basedactivating solution. Then the added chloride need tobe removed. 50 pk
IC-M10 iminodiacetate resin in the ammonium form 40µm 0.4meq/1cccartridge To remove transition metals and matrix eliminationof alkali and alkaline earth metals. 50 pk
IC-Ag/H10 It is a layered cartridge that contains IC- Ag resin and IC- H resin. 50 pk
IC-Ba/Ag/H10 It is a layered cartridge that contains IC-Ba resin, IC- Ag resin and IC- H resin. 50 pk

Phases SLF

Description

Solid supported liquid/liquid Extraction columns and plates use specially treated diatomaceous
earth materials as a solid support for liquid/liquid extractions. Agela can provide different
pH sorbents as customer requirement to make extraction of different properties substance.
This kind of material were often used in clinical analysis, it also can be used to replace
most of the analysis using Liquid/Liquid extraction (LLE).

Particles Characteristics

  • Treated diatomiteous earth materials
  • Average particle diameter: 20-80 mesh
  • pH=7 (acidification material) or 9-10 (alkalization material);
  • Capability of water absorption: 0.8-1mL/g;

The General Method Includes

  • Load an aqueous sample into the column by gravity or a soft vacuum.
  • Apply one or a multiple organic solvents by gravity or well-controlled vacuum.
  • Vacuum the organic solution which contains the analyte out from bottom of the columns or plates, collect the solution.
  • Concentrate the collected solution.

Benefit

The SPE procedures can be easily automated. It also can be used to replace most
of the analysis using Liquid/Liquid extraction to reduce the solvent usage, even
emulsification phenomenon of LLE

Sorbent Description Package Cat. No.
Cleanert SLE 80-20 mesh;pH=6-8 1000g/bottle HC1001000-7
Cleanert SLE 80-20 mesh;pH=9 1000g/bottle HC1001000-9
Cleanert SLE 80-20 mesh;pH=10 1000g/bottle HC1001000-10
Sorbent Vol. Tubes/box Special treated diatomite SLE (pH=7) Special treated diatomite SLE (pH=9)
200mg 3ml 50 HC2003-7 HC2003-9
500mg 3ml 50 HC5003-7 HC5003-9
500mg 6ml 30 HC5006-7 HC5006-9
1g 6ml 30 HC0006-7 HC0006-9
2g 12ml 20 HC200012-7 HC200012-9
4g 25ml 15 HC400025-7 HC400025-9
200mg 2ml/well 96-wellplate HC2002-7W HC2002-9W
400mg 2ml/well 96-wellplate HC4002-7W HC4002-9W
500mg 2ml/well 96-wellplate HC5002-7W HC5002-9W

Accessoires pour SPE

96well plate

Product name Specification Quality Cat.No
2mL 96w collection plate 8×12 pores Square pore and circular bottom 1 96SP2036
2mL 96w collection plate 8×12 pores Circular pore and bottom 1 96SP2036-Y
96well silica pad 8×12 pores square pore 96GP2036

12/24 Vaccum Manifold for SPE

Term Specification, Package Cat. No.
Vaccum equipment 12positions VM12
24positions VM24
Flow rate adjusting valve 12 pieces/ package A81213
Diversion needle threading the plate 12 pieces/ package A80100
Diaphragm vacuume pump 1 A01003

Positive Pressure SPE of 48 Positions (EZY-P48)

Products Name Description Cat. No.
Positive pressure SPE of 48 positions
  • deal with 48 pieces of sample at the same time
  • stable flow rate efficient for 3-mL and 6-mL minicartridge
  • pressure provided by positive pressure pump or air supply
  • safe without power supply
  • application for pretreatment on the sample of pharmacokinetics and environment
EZY-P48

Vaccum Manifold for 96 Well Plate

Term Description Cat. No.
Negative SPE with high throughput (VM96)
  • flow rate controlled by gas valve
  • display operational pressure
  • anticrrosion design
  • selective heightening modules
  • be suitable for various hydraulic plates and different eluants
VM96
Heightening module Application for the experiment of little receiving liquid VM96-001

Empty Cartridge and Sieve Plate

Cat.No Description Vol Package
AZ-IC-1 IC Empty column 1ml 100
AZ-IC-1T IC Empty column (with 2 x 20um Polyethyelene frit) 1ml 100
AZ-IC-2.5 IC Empty column 2.5ml 100
AZ-IC-2.5T IC Empty column (with 2 x 20um Polyethyelene frit) 2.5ml 100
AZ001 SPE Empty column 1ml 100
AZ003 SPE Empty column 3ml 100
AZ006 SPE Empty column 6ml 100
AZ010 SPE Empty column 10ml 100
AZ012 SPE Empty column 12ml 100
AZ030 SPE Empty column 30ml 100
AZ060 SPE Empty column 60ml 50
AZ150 SPE Empty column 150ml 25
LAZ010 Large Reservoir Capacity SPE column 10ml 100
AS001-A SPE 20um Polyethyelene Frit 1ml 100
AS003-A SPE 20um Polyethyelene frit 3ml 100
AS006-A SPE 20um Polyethyelene frit 6ml 100
AS010-A SPE 20um Polyethyelene frit 10ml 100
AS012-A SPE 20um Polyethyelene frit 12ml 100
AS030-A SPE 20um Polyethyelene frit 30ml 100
AS060-A SPE 20um Polyethyelene frit 60ml 50
AS150-A SPE 20um Polyethyelene frit 150ml 25
LAS010-A Large Reservoir Capacity SPE 20um Polyethyelene frit 10ml 100
A80115 SPE adaptor fit 1,3,6,12ml 12
96SP2036 Collection plate, square well, round bottom 8×12well 24
96SP2036-Y Collection plate, round well,round bottom 8×12well 24
96GP2036 96 well cap mat 8×12well 24
96CD1025 96 well crash and protein precipitate filter plate 1ml/well 2
96CD2025 96 well crash and protein precipitate filter plate (Use Vacuum or Pressure for Elution) 2ml/well 2
96CD2025-F 96 well crash and protein precipitate filter plate (Use Centrifugation For Elution) 2ml/well 2
96CD01 Crash and protein precipitate filter cartridge 1ml 1ml 100

Cleanert, la SPE de Qualité !

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